RE: Correcting for salt vs. base

From: Steven Troy Date: March 26, 2014 technical Source: mail-archive.com
Hi Dennis, In my experience, most (but not all) doses are expressed as mg of free base, eg, 0.5mg anagrelide (as 0.61mg of anagrelide*HCl). This facilitates changing salt forms where the dose of free base may be unchanged while the dose of the salt form will vary based on the size of the salt. I try to reinforce this approach with my CMC colleagues whenever possible to ensure consistency. However, I agree with you that calculation of clearance and volume should be based on mg of the administered free-base in cases where the dose is expressed as mg of the salt form. Best regards, Steve Steven M. Troy Clinical Pharmacology and Pharmacokinetics Shire 725 Chesterbrook Boulevard Wayne, PA 19087-5637 USA Office: +1 (484) 595 8780 Mobile/Cell +1 (484) 375 3692 [email protected]<mailto:[email protected]> http://www.shire.com
Quoted reply history
From: [email protected] [mailto:[email protected]] On Behalf Of Fisher Dennis Sent: Wednesday, March 26, 2014 8:57 AM To: [email protected] Subject: [NMusers] Correcting for salt vs. base Colleagues I have been troubled by a minor issue for some time. Consider the following situation: Dose is reported in mg salt Cp is reported in ng/ml base Since CL is dose / AUC and AUC is merely the integral of Cp vs. time, in theory, dose should be converted to mg base (or concentration to ng/ml salt). However, I am not sure if everyone does that. In fact, an argument against it is that not doing the conversion permits one to relate the administered dose (which is usually based on salt) to a Cp value (usually based on base). I am interested to hear what approach people use. Dennis Dennis Fisher MD P < (The "P Less Than" Company) Phone: 1-866-PLessThan (1-866-753-7784) Fax: 1-866-PLessThan (1-866-753-7784) http://www.plessthan.com/ ****************************************************** Shire plc, the ultimate parent of the Shire Group of companies, is registered in Jersey No. 99854 Registered Office: 22 Grenville Street, St Helier, Jersey JE4 8PX ****************************************************** Please consider the environment before printing this e-mail This email and any files transmitted with it are confidential and may be legally privileged and are intended solely for the use of the individual or entity to whom they are addressed. If you are not the intended recipient please note that any disclosure, distribution, or copying of this email is strictly prohibited and may be unlawful. If received in error, please delete this email and any attachments and confirm this to the sender.
Mar 26, 2014 Fisher Dennis Correcting for salt vs. base
Mar 26, 2014 Siv Jönsson RE: Correcting for salt vs. base
Mar 26, 2014 Brian Sadler RE: Correcting for salt vs. base
Mar 26, 2014 Paul Hutson Re: Correcting for salt vs. base
Mar 26, 2014 Steven Troy RE: Correcting for salt vs. base
Mar 26, 2014 Edmund Capparelli Re: Correcting for salt vs. base
Mar 26, 2014 Jeroen Elassaiss-Schaap RE: Correcting for salt vs. base
Mar 27, 2014 Nancy Sambol Re: Correcting for salt vs. base