help on diagnostic of a problem -- about M3 method for LLOQ:

From: Ethan Wu Date: February 11, 2010 technical Source: mail-archive.com
Dear users, I am working on a dataset with not small percentage below LLOQ. when I implemented M3 method to account for this, I always getting this error message: 0PROGRAM TERMINATED BY OBJ ERROR IN CLIK WITH INDIVIDUAL 2 ID=0.19000000E+02 CONDITIONAL LIKELIHOOD FOR SOME OBSERVATION ESTIMATED TO BE NEGLIGIBLE note that ID 19 is the first subject in the dataset. this is how I specify the $ERR (a combinative erro) and $EST: __________ $ERROR IPRED = F IRES = DV-IPRED FLAG=1 IF(STDY.GT.3) FLAG=0 DEL=0 W = SQRT(THETA(7)**2*FLAG+THETA(8)**2*(1-FLAG)+THETA(9)**2*IPRED**2) IF(W.EQ.0)DEL=1 IWRES = IRES/(W+DEL) IF (TYPE.EQ.2.AND.CMT.EQ.2) DUM=(LOQ-IPRED)/(THETA(7)**2*FLAG+THETA(8)**2*(1-FLAG)+THETA(9)**2*IPRED**2) CUMD=PHI(DUM) IF (TYPE.EQ.2) THEN F_FLAG=1 Y=CUMD ENDIF IF (TYPE.EQ.1) THEN F_FLAG=0 Y = IPRED+W*EPS(1) ENDIF $ESTIMATION METHOD=1 LAPLACIAN MAXEVAL=9999 PRINT=10 NOABORT or this: $ESTIMATION METHOD=1 INT LAPLACIAN MAXEVAL=9999 PRINT=10 NOABORT _____ Interstingly, when I use Log-transformed data, the model would run fine. this is how I specify $ERR (an additive error) and $EST, all the other aspects of model are the same between two tries. Could someone help me understand what is happening? Thanks. _____ $ERROR DEL = 0 IF(F.LE.0) DEL = 1 IPRED = LOG(F+DEL) IRES = DV-IPRED FLAG=1 IF(STDY.GT.3) FLAG=0 W = SQRT(THETA(7)**2*FLAG+THETA(8)**2*(1-FLAG)) DEL1=0 IF(W.EQ.0)DEL1=1 IWRES = IRES/(W+DEL1) IF (TYPE.EQ.2.AND.CMT.EQ.2) DUM = (LOG(LOQ)-IPRED)/(THETA(7)*FLAG+THETA(8)*(1-FLAG)) CUMD=PHI(DUM) IF (TYPE.EQ.2) THEN F_FLAG=1 Y=CUMD ENDIF IF (TYPE.EQ.1) THEN F_FLAG=0 Y=IPRED +EPS(1)*W ENDIF $ESTIMATION METHOD=1 LAPLACIAN MAXEVAL=9999 PRINT=10 NOABORT
Feb 11, 2010 Ethan Wu help on diagnostic of a problem -- about M3 method for LLOQ:
Feb 11, 2010 Jae Eun Ahn RE: help on diagnostic of a problem -- about M3 method for LLOQ: